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基于绿色超分子溶剂的微提取方法,使用自然存在的成分进行蔬菜中的真菌杀菌剂的色谱测定

Ramil Afzaletdinov¹, Aleksei Pochivalov², Sergey Garmonov³

¹Department of Analytical Chemistry, Saint Petersburg State University, Universitetskaya Emb. 7/9, 199034 St. Petersburg, Russia; Department of Analytical Chemistry, Certification and Quality Management, Kazan National Research Technological University, Karl Marx street 68, 420015 Kazan, Russia.

Journal of chromatography. A

|March 2, 2026

概括

一种新的绿色微提取方法使用甲基糖化物和林纳醇有效地从蔬菜中提取本齐米达杀菌剂. 这种方法为 thiabendazole 和 carbendazim 确定提供了高回收率.

科学领域:

分析化学分析化学
绿色化学绿色化学

背景情况:

像 thiabendazole 和 carbendazim 这样的西米达杀菌剂在农业中被广泛使用.
准确而敏感的检测方法对于监测食品中的杀菌剂残留物至关重要.
现有的方法可能涉及强化学品或复杂的程序.

研究的目的:

开发一种基于高分子溶剂的绿色微提取技术,用于农业杀剂.
利用自然存在的成分来提高目标分析物的预度.
在蔬菜样本中测定 thiabendazole 和 carbendazim.

主要方法:

从二甲基葡萄糖和林纳醇开发一种超分子溶剂.
从植物基质中微提取 thiabendazole 和 carbendazim.
使用高性能液态色谱与光检测进行分析.

主要成果:

使用林纳醇获得的高提取回收率 (>98%) 和丰富系数.
在土豆,甜菜和生中成功确定了 thiabendazole 和 carbendazim.
达到低检测极限 (0.5微克千克-1对于蒂亚本达,4微克千克-1对于卡尔本达).
证明了良好的精度,相对标准偏差≤6%.

结论:

建立了一种绿色和高效的微提取方法,使用天然衍生的超分子溶剂.
该技术适用于在蔬菜中敏感确定本齐米达杀菌剂.
这种方法突显了基多糖化物和化物的分析化学潜力.

关键词:

西米达的杀菌剂西米达的杀菌剂甲基甲基甲基糖化物是什么?高性能液体色谱与光检测检测.林娜洛尔 (Linalool) 是一个名为林娜洛尔 (Linalool) 的名字.微提取微提取微提取这是一种超分子溶剂.

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