Related Experiment Video
Updated: Jul 24, 2026

Preparation and Testing of Plant Seed Meal-based Wood Adhesives
Published on: March 5, 2015
The effect of a re-wetting agent on dentin bonding
J Perdigão1, B Van Meerbeek, M M Lopes
1Department of Operative Dentistry, School of Dentistry, University of North Carolina at Chapel Hill 27599-7450, USA. jorge_perdigao@dentistry.unc.edu
Re-wetting dried dentin with a hydroxyethyl methacrylate (HEMA) aqueous solution restores dentin bond strengths and resin infiltration. This method effectively compensates for collagen network collapse caused by drying, crucial for simplified one-bottle dental adhesives.
Area of Science:
- Dental Materials Science
- Adhesive Dentistry
- Biomaterials Engineering
Background:
- New simplified one-bottle dentin bonding systems are sensitive to substrate moisture.
- Understanding moisture effects on dentin surface is critical for optimal bonding.
Purpose of the Study:
- To compare dentin bond strengths and interfacial morphology of three one-bottle bonding systems.
- To evaluate the effect of re-wetting dried dentin with a hydroxyethyl methacrylate (HEMA) aqueous solution on bond strength and resin impregnation.
Main Methods:
- Three one-bottle dentin bonding systems were tested on three etched dentin surface conditions: moist, dried, and re-moistened with HEMA solution.
- Shear bond strengths were analyzed using ANOVA.
- Resin-dentin interfaces were examined using transmission and scanning electron microscopy.
Main Results:
- Drying dentin significantly decreased bond strengths and resulted in incomplete resin infiltration of the collagen network.
- Re-wetting dried dentin with HEMA solution restored bond strengths to levels comparable to moist dentin.
- HEMA re-wetting improved the resin impregnation of the collagen network, increasing interfibrillar space.
Conclusions:
- Aqueous HEMA solution can effectively compensate for dentin surface dryness induced by air-drying after etching.
- The water content in some current ethanol- and water-based adhesives may be insufficient to prevent collagen network collapse upon drying.
Related Concept Videos
EDTA: Auxiliary Complexing Reagents
Effects of EDTA on End-Point Detection Methods
In the visual method, metal-ion indicators (metallochromic dyes), which have distinct colors in their free and complex forms, are added to the mixture to signal the titration's end point. They form stable complexes with metal ions, but these complexes are weaker than the corresponding metal–EDTA complexes. As a result, EDTA...
Mortar Properties
Bonding and Strength of Aggregate
Porosity and Absorption of Aggregate
When all pores in an aggregate are filled with water, the aggregate is considered saturated and surface-dry. If left in dry air, water will evaporate until the aggregate...
Drying Shrinkage
A portion of this drying shrinkage can be reversed; if the concrete is...

