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An efficient one-pot method for the large-quantitative production of radiopharmaceutical ligand: diazadioximes
H J Ding1, Y F Huang, C C Tzeng
1Department of Nuclear Medicine, School of Technology for Medical Sciences, Kaohsiung Medical University, Taiwan, R.O.C.
Chemical & Pharmaceutical Bulletin
|March 8, 2000
Abstract:
An efficient one-pot procedure for the preparation of diazadioxime was described. Treatment of ketooximes with alkyldiamine followed by NaBH4 in dry ethanol afforded the corresponding d,l-diazadioximes in 56--74% yield without isolation of the intermediates.