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Na3Co(NO2)6 at 293 and 10 K.

B N Figgis1, A N Sobolev

  • 1Chemistry Department, University of Western Australia, 35 Stirling Highway, Crawley WA 6009, Australia. bnf@crystal.uwa.edu.au

Acta Crystallographica. Section C, Crystal Structure Communications
|August 11, 2001
PubMed
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The crystal structure of trisodium hexanitrocobaltate(III) was determined using X-ray diffraction. This study reveals a distorted octahedral cobalt-nitrite anion, providing data for charge-density analysis.

Area of Science:

  • Inorganic chemistry
  • Solid-state chemistry
  • Crystallography

Background:

  • Trisodium hexanitrocobaltate(III) is an inorganic coordination compound.
  • Understanding the precise atomic arrangement is crucial for its chemical properties.

Purpose of the Study:

  • To determine the crystal structure of trisodium hexanitrocobaltate(III) at two different temperatures.
  • To provide high-quality crystallographic data for potential charge-density studies.

Main Methods:

  • X-ray diffraction was employed to analyze the crystal structure.
  • Data collection was performed at 293 K (room temperature) and 10 K (low temperature).

Main Results:

  • The crystal structure was successfully determined, revealing a distorted octahedral coordination geometry for the hexanitrocobaltate(III) anion (Co(NO2)6(3-)).

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  • Accurate and extensive crystallographic data sets were obtained at both temperatures.

    • Conclusions:

    • The determined structure provides a detailed understanding of trisodium hexanitrocobaltate(III).
    • The collected data is suitable for advanced analyses, such as charge-density studies, furthering insights into chemical bonding.