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Rinneite, K(3)Na[FeCl(6)], at 293, 84 and 9.5 K.

B N Figgis1, A N Sobolev, E S Kucharski

  • 1Chemistry Department, University of Western Australia, Nedlands, WA 6907, Australia.

Acta Crystallographica. Section C, Crystal Structure Communications
|July 21, 2004
PubMed
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Researchers determined the crystal structure of tripotassium sodium hexachloroferrate(II) using X-ray diffraction at various temperatures. The collected data is suitable for detailed charge-density analysis.

Area of Science:

  • Inorganic Chemistry
  • Solid-State Chemistry
  • Crystallography

Background:

  • Hexachloroferrate(II) compounds are of interest due to their magnetic and structural properties.
  • Understanding the precise atomic arrangement is crucial for predicting material behavior.

Purpose of the Study:

  • To determine the crystal structure of tripotassium sodium hexachloroferrate(II).
  • To provide high-quality crystallographic data for further analysis.

Main Methods:

  • X-ray diffraction was employed to study the crystal structure.
  • Data collection was performed at three different temperatures: 293 K, 84 K, and 9.5 K.

Main Results:

  • The crystal structure of tripotassium sodium hexachloroferrate(II) was successfully determined.

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  • Accurate and extensive crystallographic data sets were obtained at cryogenic temperatures.

    • Conclusions:

    • The obtained data is well-suited for advanced charge-density analysis.
    • This study provides a foundational structural understanding of this specific hexachloroferrate(II) salt.