[Determination of eight trichothecene mycotoxins using GCMSMS methods. I. elaboration of MS/MS conditions]
Agnieszka Filipek1, Marek Daniewski, Karol Bal
1Samodzielna Pracownia Technologii Zywności i Zywienia Instytut Zywności i Zywienia 02-903 Warszawa, ul. Powsińska 61/63.
Abstract:
Trichothecene mycotoxins are commonly distributed in cereals in the world. Rapid and accurate methods for the determination of these toxins are required to prevent the intoxication of human and to contribute to the supply of safe foods and feed. MSMS mode was applied for identification of eight trichothecene mycotoxins with Finnigan/Mat GCQ GC/MS system. We describe here optimal parameters of CID and to obtain best pairs of ions (precursor ions and daughter ions) for all analysed toxins.
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