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Updated: Aug 22, 2026
Analysis of Organochlorine Pesticides in a Soil Sample by a Modified QuEChERS Approach Using Ammonium Formate
Published on: January 20, 2023
Liquid chromatographic determination of novel aminithiazolecarboxamide fungicide residues in soil and crops using
Byoung-Hyoun Kim1, Jong Hoa Ok
1Analytical Science, Corporate R&D/LG Chemical Research Park, LG Chemical Ltd., 104-1, Moonji-dong, Yusong-gu, Daejeon, 305-380, South Korea. bhkime@lgchem.com
Abstract:
A simple and convenient liquid chromatographic method has been developed and applied to the analysis of the novel aminothiazolecarboxamide fungicide, ethaboxam, in soil and crops. After the isolation and concentration of analyte from soil and crops, clean-up and separation of sample solutions are performed by high-performance liquid chromatography with online solid-phase extraction. Good linearity (r2 > 0.9995), recovery [for soil, 95.3-98.4%, and crops (grape, red pepper), 92.9-95.9%], and repeatability are achieved in the calibration range of 0.1-10.3 microg/mL. The limit of detection is the 2.5 parts per billion (ppb) (40 g of soil) and the 20 ppb (25 g of crops), respectively. This assay method shows the suitability for the residual analysis of ethaboxam in soil and crops.
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