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Structure and Coordination Determination of Peptide-metal Complexes Using 1D and 2D 1H NMR
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Published on: December 16, 2013

Conformational evaluation and detailed 1H and 13C NMR assignments of eremophilanolides

Eleuterio Burgueño-Tapia1, Luis R Hernández, Adriana Y Reséndiz-Villalobos

  • 1Departamento de Química, Unidad Profesional Interdisciplinaria de Biotecnología, Instituto Politécnico Nacional, Av. Acueducto s/n, La Laguna Ticomán, México D.F., 07340 Mexico. eburgenio@acei.upibi.ipn.mx

Magnetic Resonance in Chemistry : MRC
|September 15, 2004
PubMed

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¹³C NMR: Distortionless Enhancement by Polarization Transfer (DEPT)

When proton-coupled carbon-13 spectra are simplified by a broadband proton decoupling technique, structural information about the coupled protons is lost. Distortionless enhancement by polarization transfer (DEPT) is a technique that provides information on the number of hydrogens attached to each carbon in a molecule. While the DEPT experiment utilizes complex pulse sequences, the pulse delay and flip angle are specifically manipulated. The resulting signals have different phases depending on...
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