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Updated: Aug 21, 2026

Evaluation of the Curing of Adhesive Systems by Rheological and Thermal Testing
Published on: July 3, 2020
Color stability of acrylic resin adhesives with different initiation modes
Naomi Tanoue1, Yoshikazu Koishi, Hiroaki Yanagida
1Department of Specialized Dentistry, Nagasaki University Hospital of Medicine and Dentistry, Japan. t-naomi@net.nagasaki-u.ac.jp
Abstract:
The purpose of this study was to evaluate the color stability of two acrylic resin adhesives with different activation systems: a benzoyl peroxide (BPO)-amine redox system and a tri-n-butylborane (TBB) derivative system. The colorimetric values of the two resins in different shades (Clear and Ivory) were determined (n=5) 24 hours after polymerization as a baseline using the L*a*b* system of the Commission Internationale de l'Eclairage (CIE). The specimens were thereafter immersed in distilled water, and the color difference (deltaE*) values were calculated. After 24 weeks, the TBB-initiated material showed a significantly (p<0.05) lower color change than the BPO-amine-initiated material. The deltaE* values for the BPO-amine-initiated materials were 6.9 for Clear and 15.8 for Ivory, whereas those for the TBB-initiated materials were 1.3 and 1.8 respectively. Thus, it was concluded that the TBB-initiated material had superior color stability to that of the BPO-amine-initiated material.
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