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Synthesis of 1,10-N,N'-phenanthroline dioxides using HOF.CH(3)CN complex
1School of Chemistry, Raymond and Beverly Sackler Faculty of Exact Sciences, Tel-Aviv University, Tel-Aviv 69978, Israel.
The Journal of Organic Chemistry
|March 12, 2005
Abstract:
[reaction: see text] HOF.CH(3)CN, a very efficient oxygen-transfer agent, made readily from F(2), H(2)O, and CH(3)CN, was reacted with various 1,10-phenanthroline derivatives to form the corresponding N,N'-dioxides in good yields and short reaction times.