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Visualization of grain subdivision by analysing the misorientations within a grain using electron backscatter
S Van Boxel1, M Seefeldt, B Verlinden
1Department of Metallurgy and Materials Engineering (MTM), Katholieke Universiteit Leuven, Kasteelpark Arenberg 44, B-3001 Heverlee, Belgium. steven.vanboxel@mtm.kuleuven.ac.be
This study analyzes grain misorientation using electron backscatter diffraction (EBSD), introducing a new visualization technique for misorientation band structures and validating grain boundary reconstruction methods.
Area of Science:
- Materials Science
- Crystallography
- Electron Microscopy
Background:
- Understanding grain misorientation is crucial for materials properties.
- Electron Backscatter Diffraction (EBSD) is a key technique for microstructural analysis.
- Deformation processes significantly influence grain orientation and structure.
Purpose of the Study:
- To analyze grain and point-to-point misorientation in deformed materials using EBSD data.
- To introduce and discuss a novel visualization technique for misorientation band structures.
- To compare grain boundary reconstruction methods and validate their accuracy using confidence index maps.
Main Methods:
- Detailed analysis of misorientation angle and axis from EBSD datasets.
- Development of a new color-mapping technique to visualize grain subdivision structures.
- Comparison of grain boundary reconstruction algorithms against EBSD confidence index maps.
Main Results:
- Visualization of misorientation relative to average grain orientation and along lines within deformed grains.
- Demonstration of the significance of misorientation axis monitoring in identifying band structures.
- Validation of grain boundary reconstruction accuracy through confidence index mapping.
Conclusions:
- The study provides enhanced methods for analyzing and visualizing grain misorientation and substructures.
- The new visualization technique effectively highlights misorientation band structures.
- The comparison of reconstruction methods offers a validation pathway for EBSD data processing.
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