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Optimization of isotope-labeling conditions for lambertellin based on isotope patterns observed by mass spectrometry
Takanori Murakami1, Akane Sasaki, Eri Fukushi
1Faculty of Agriculture and Life Science, Hirosaki University, 3-Bunkyo-cho, Hirosaki 036-8561, Japan.
Bioorganic & Medicinal Chemistry Letters
|May 3, 2005
Abstract:
A method for the sensitive analysis of the incorporation level of labeled acetate was developed. This method allowed for the optimization of the conditions for lambertellin with up to 48% average incorporation of labeled acetate.
