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Related Experiment Videos

X-ray diffractometer combining synchrotron radiation and pulsed magnetic fields up to 40 T.

Y Narumi1, K Kindo, K Katsumata

  • 1ISSP, University of Tokyo, Kashiwa, Chiba 277-858, Japan. narumio@issp.u-tokyo.ac.jp

Journal of Synchrotron Radiation
|April 29, 2006
PubMed
Summary

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A new synchrotron X-ray diffractometer with a 40 Tesla pulsed field magnet was developed. This instrument observed field-dependent lattice distortion in cobalt oxide (CoO) up to 38 T.

Area of Science:

  • Condensed Matter Physics
  • Materials Science
  • Instrumentation

Background:

  • High magnetic fields are crucial for studying material properties.
  • Existing equipment may have limitations in field strength or experimental integration.
  • Synchrotron X-ray diffraction provides atomic-level structural information.

Purpose of the Study:

  • To develop and describe a novel synchrotron X-ray diffractometer integrated with a high-field pulsed magnet.
  • To demonstrate the instrument's capability in probing field-induced structural changes.
  • To investigate magnetostriction effects in materials under extreme magnetic fields.

Main Methods:

  • Development of a pulsed field magnet (up to 40 T) with a 3 mm gap for X-ray passage.
  • Utilizing a PILATUS 100K pixel detector for recording X-ray diffraction patterns.

Related Experiment Videos

  • Performing X-ray diffraction measurements on a cobalt oxide (CoO) powder sample below its Néel temperature.
  • Main Results:

    • Successful integration of a 40 T pulsed field magnet with a synchrotron X-ray diffractometer.
    • Observation of field-dependent lattice distortion in CoO up to 38 T.
    • Demonstration of the instrument's sensitivity to magnetostriction effects.

    Conclusions:

    • The developed instrument is capable of performing high-field X-ray diffraction studies.
    • Significant magnetostriction effects were observed in CoO under high magnetic fields.
    • This new capability opens avenues for exploring other materials under extreme conditions.