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Published on: December 15, 2015

Feng Gao1, Yilin Wang, Wilfred T Tysoe

  • 1Department of Chemistry and Biochemistry, and Laboratory for Surface Studies, University of Wisconsin-Milwaukee, Milwaukee, WI 53211, USA.

Journal of the American Chemical Society
|May 25, 2006
PubMed

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The radical dimerization of ketones or aldehydes gives vicinal diols through a pinacol coupling reaction. However, the behavior of titanium metals used for the reaction as a source of electrons is unusual. When the reaction is carried out in the presence of titanium, diols can be isolated at low temperatures. Else titanium further reacts with diols, forming alkenes through the McMurry reaction.