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Trimorphism in solid resorcinarenes.

Charles J M Stirling1, L Johan Fundin, Nicholas H Williams

  • 1Centre for Chemical Biology, Department of Chemistry, University of Sheffield, Sheffield, U.K. S3 7HF. C.Stirling@Sheffield.ac.uk

Chemical Communications (Cambridge, England)
|April 26, 2007
PubMed
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Nonylresorcinarene exhibits three distinct phases—layer, hexamer, and amorphous—which are in thermal equilibrium. This behavior contrasts with methylresorcinarene and nonylpyrogallene.

Area of Science:

  • Supramolecular Chemistry
  • Materials Science

Background:

  • Resorcinarene derivatives are known for their unique structural properties.
  • Understanding phase behavior is crucial for designing novel materials.

Purpose of the Study:

  • To investigate the distinct phases of nonylresorcinarene.
  • To compare the phase behavior of nonylresorcinarene with related compounds like methylresorcinarene and nonylpyrogallene.

Main Methods:

  • Isolation and characterization of different nonylresorcinarene phases.
  • Thermal analysis to determine phase equilibrium.

Main Results:

  • Nonylresorcinarene was found to exist in three isolable phases: a layer structure, a hexamer, and an amorphous phase.
  • These three phases were determined to be in thermal equilibrium.

Related Experiment Videos

  • This phase behavior is unique to nonylresorcinarene when compared to methylresorcinarene and nonylpyrogallene.

    • Conclusions:

    • Nonylresorcinarene displays complex phase polymorphism.
    • The thermal equilibrium between its distinct phases offers opportunities for controlled material design.