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Updated: Jul 12, 2026

Energy Dispersive X-ray Tomography for 3D Elemental Mapping of Individual Nanoparticles
Published on: July 5, 2016
Three-dimensional chemical mapping by scanning transmission X-ray spectromicroscopy
Göran A Johansson1, Tolek Tyliszczak, Gary E Mitchell
1Department of Chemistry and BIMR, McMaster University, Hamilton, Canada L8S 4M1. gajonsson@lbl.gov
Abstract:
Three-dimensional (3-d) chemical mapping using angle-scan tomography in a scanning transmission X-ray microscope is demonstrated. Apparatus, experimental procedures and data processing are presented and the 3-d spatial resolution is evaluated. The technique is illustrated using mapping of a low-density acrylate polyelectrolyte in and outside of polystyrene microspheres dispersed in water in a 4 microm-diameter microcapillary. The 3-d chemical visualization provides information about the microstructure that had not previously been observed.
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