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Updated: Jul 9, 2026

Processing of Bulk Nanocrystalline Metals at the US Army Research Laboratory
Published on: March 7, 2018
Annealing characteristics of nanostructured Cu-Fe-P alloy processed by accumulative roll-bonding
Seong-Hee Lee1, Chung-Hyo Lee, Suk-Ja Yoon
1Department of Advanced Materials Science and Engineering, Mokpo National University, Muan-gun 534-729, Chonnam, Korea.
Abstract:
Annealing characteristics of a nanostructured copper alloy processed by accumulative roll-bonding (ARB) were studied. A nano-grained Cu-Fe-P alloy processed by 8 cycles of the ARB was annealed at various temperatures ranging from 100 to 400 degrees C for 0.6 ks. The sample still showed an ultrafine grained (UFG) structure up to 250 degrees C, however above 300 degrees C it began to replace by equiaxed and coarse grains due to an occurrence of the conventional static recrystallization. The hardness of the annealed copper decreased largely above 300 degrees C. These annealing characteristics of the UFG copper alloy were compared to those of a high purity copper.

