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Related Concept Videos

Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation01:26

Inductively Coupled Plasma Atomic Emission Spectroscopy: Instrumentation

Inductively coupled plasma (ICP) is the common plasma source used in atomic emission spectroscopy (AES), a technique that detects and analyzes various elements in a sample. This method is often called inductively coupled plasma atomic emission spectroscopy (ICP-AES).
There are three main types of inductively coupled plasma atomic emission spectroscopy  (ICP-AES) instruments: sequential, simultaneous multichannel, and Fourier transform instruments, with the latter being less commonly used.
Atomic Absorption Spectroscopy: Radiation and Light Sources01:13

Atomic Absorption Spectroscopy: Radiation and Light Sources

Atomic absorption spectroscopy (AAS) relies on the Beer-Lambert law, which requires that the radiation source emits a narrow range of wavelengths to match the absorption characteristics of the analyte atom. The primary criteria for choosing an appropriate radiation source in AAS is to provide a precise and intense emission at specific wavelengths that will allow accurate detection of the analyte.
Two common narrow-range 'line' sources used in AAS are hollow-cathode lamps (HCLs) and...
Atomic Absorption Spectroscopy: Instrumentation01:22

Atomic Absorption Spectroscopy: Instrumentation

An atomic absorption spectrophotometer (AAS) comprises several components: a radiation source, an atomizer, a monochromator, and a detector. The radiation source can be a hollow-cathode lamp (HCL) or an electrodeless-discharge lamp (EDL), both of which provide a narrow emission line of the required wavelength. However, some instruments use continuum sources and high-resolution monochromators to achieve a narrow range of radiation.
The atomizer used in AAS can be either a flame atomizer or an...
Atomic Emission Spectroscopy: Instrumentation01:22

Atomic Emission Spectroscopy: Instrumentation

The instrumentation of atomic emission spectrometry (AES) involves various components, including atomization devices that convert samples into gas-phase atoms and ions. There are two main types of atomization devices: continuous and discrete atomizers.  Continuous atomizers, like plasmas and flames, introduce samples in a constant stream, while discrete atomizers inject individual samples using syringes or autosamplers. The most common discrete atomizer is the electrothermal atomizer.
X-ray Imaging01:24

X-ray Imaging

German physicist Wilhelm Röntgen (1845–1923) was experimenting with electrical current when he discovered that a mysterious and invisible "ray" would pass through his flesh but leave an outline of his bones on a screen coated with a metal compound. In 1895, Röntgen made the first durable record of the internal parts of a living human: an "X-ray" image (as it came to be called) of his wife’s hand. Scientists worldwide quickly began their own experiments with X-rays, and by 1900, X-ray was widely...
Atomic Fluorescence Spectroscopy01:29

Atomic Fluorescence Spectroscopy

Atomic fluorescence spectroscopy (AFS) is an analytical technique that involves the electronic transitions of atoms in a flame, furnace, or plasma being excited by electromagnetic (EM) radiation. When these atoms absorb energy, they become excited and subsequently release energy as they return to their original state. This emitted light, or "fluorescence," is observed at a right angle to the incident beam. Both absorption and emission processes transpire at distinct wavelengths, which are...

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Measurement of X-ray Beam Coherence along Multiple Directions Using 2-D Checkerboard Phase Grating
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A Geiger-mode avalanche photodiode array for X-ray photon correlation spectroscopy.

I Johnson1, Z Sadygov, O Bunk

  • 1Paul Scherrer Institut, 5232 Villigen PSI, Switzerland. ian.johnson@psi.ch

Journal of Synchrotron Radiation
|December 20, 2008
PubMed
Summary

A new X-ray detector system enables advanced X-ray photon correlation spectroscopy (XPCS) studies. This system measures temporal fluctuations in diffraction patterns, offering insights into material dynamics across Hz to kHz frequencies.

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Area of Science:

  • Materials Science
  • Condensed Matter Physics
  • Photonics

Background:

  • X-ray photon correlation spectroscopy (XPCS) is a powerful technique for probing dynamic processes in materials.
  • Studying dynamics in the Hz to kHz frequency range is crucial for understanding various physical phenomena.
  • Existing detector systems may have limitations in speed or resolution for certain XPCS applications.

Purpose of the Study:

  • To develop and demonstrate a novel two-dimensional detector system for X-ray photon correlation spectroscopy (XPCS).
  • To enable the investigation of system dynamics within the frequency range of several Hz to kHz.
  • To provide a detailed account of the components and performance of the new detector system.

Main Methods:

  • Development of a two-dimensional detector system.
  • Integration of a thin 100 micrometer scintillation crystal with a Geiger-mode avalanche photodiode array.
  • Characterization of the detector's performance for XPCS measurements.

Main Results:

  • Successful construction and demonstration of a novel 2D detector for XPCS.
  • The detector system is capable of measuring fluctuations in the Hz to kHz frequency range.
  • The system combines a scintillation crystal with a Geiger-mode avalanche photodiode array for enhanced performance.

Conclusions:

  • The developed X-ray detector system is suitable for advanced XPCS studies.
  • This technology opens new avenues for investigating material dynamics at intermediate timescales.
  • The detailed description facilitates the replication and further development of such detector systems.