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Updated: Jun 25, 2026
High-resolution Tandem Mass Spectrometry for Studying Chemical Constituents of Gynura bicolor DC
Published on: February 2, 2024
[Studies on chemical constituents from leaves of Lysidice brevicalyx]
Hua-liang Yang1, Shi-shan Yu, Yue-hu Pei
1Key Laboratory of Bioactive Substances and Resources Utilization of Chinese Herbal Medicine, Institute of Materia Medica, Peking Union Medical College and Chinese Academy of Medical Sciences, Beijing 100050, China.
Objective:
To study the chemical constituents of Lysidice brevicalyx.
Method:
Various chromatographic techniques were used to isolate and purify the constituents such as column chromatography on silica gel, Rp-silica gel, Sephadex LH-20 and HPLC. The structures were elucidated by chemical evidence and spectroscopic methods.
Result:
Seven compounds were isolated from the 95% ethanol extract of the leaves of L. brevicalyx and these compounds were elucidated as 2-0-[1-(3-methylbutyryl)phloroglucin-ol]-beta-D-glucopynanoside (1), 3-beta-D-glucopyranosyloxy-4, 5-dimethoxy-benzoic acid (2), benzyl alcohol O-beta-D-glucopyra noside (3), polydatin (4), quercetin-3-alpha-L-rhamnopyranoside (5), ethyl gallate (6), benzyl 6-O-alpha-L-arabinofurano syl-beta-D-glucopynanoside (7).
Conclusion:
All Compounds were isolated from this plant for the first time. Compounds 2, 3, 5-7 were obtained from this genus for the first time.
