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Toward ultrafast time-resolved Debye-Scherrer x-ray diffraction using a laser-plasma source.

U Shymanovich1, M Nicoul, W Lu

  • 1Institut für Experimentelle Physik, Universität Duisburg-Essen, Lotharstr. 1, 47048 Duisburg, Germany. uladzimir.shymanovich@uni-due.de

The Review of Scientific Instruments
|September 4, 2009
PubMed
Summary
This summary is machine-generated.

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An elliptical glass capillary focuses ultrashort X-ray pulses from laser-produced plasmas. This enables Debye-Scherrer diffraction experiments, expanding time-resolved X-ray diffraction capabilities for diverse materials.

Area of Science:

  • Physics
  • Materials Science
  • Optics

Background:

  • Femtosecond laser-produced plasmas generate ultrashort X-ray pulses.
  • Focusing these divergent X-ray pulses is crucial for advanced applications.
  • Existing methods may limit the range of materials for time-resolved studies.

Purpose of the Study:

  • To demonstrate the focusing of ultrashort X-ray pulses using an elliptical glass capillary.
  • To apply this focused X-ray beam to Debye-Scherrer diffraction experiments.
  • To expand the applicability of time-resolved X-ray diffraction to a wider range of materials.

Main Methods:

  • Utilizing an elliptical glass capillary optic with 7x magnification.
  • Focusing ultrashort Copper K alpha (Cu Kα) X-ray pulses from a femtosecond laser-plasma source.

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  • Performing Debye-Scherrer diffraction experiments with simultaneous detection of multiple diffraction orders.

    • Main Results:

    • Achieved a quasicollimated X-ray beam with a divergence of 0.18 degrees.
    • Successfully demonstrated Debye-Scherrer diffraction using the focused X-ray pulses.
    • Enabled simultaneous detection of several diffraction orders.

    Conclusions:

    • Elliptical glass capillaries are effective for focusing ultrashort X-ray pulses from laser-produced plasmas.
    • This technique facilitates time-resolved Debye-Scherrer diffraction experiments.
    • The method broadens the scope of time-resolved X-ray diffraction for materials not readily available as single crystals.