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Preparation of Silica Nanoparticles Through Microwave-assisted Acid-catalysis
Published on: December 16, 2013
Functional silica nanoparticles synthesized by water-in-oil microemulsion processes
Tangi Aubert1, Fabien Grasset, Stéphane Mornet
1Université de Rennes 1, UMR, Science Chimiques de Rennes, UR1-CNRS 6226, Equipe Chimie du Solide et Matériaux, Campus de Beaulieu, CS 74205, F-35042 Rennes Cedex, France.
Abstract:
Water-in-oil (W/O) microemulsion is a well-suitable confined reacting medium for the synthesis of structured functional nanoparticles of controlled size and shape. During the last decade, it allowed the synthesis of multi-functional silica nanoparticles with morphologies as various as core-shell, homogenous dispersion or both together. The morphology and properties of the different intermediates and final materials obtained through this route are discussed in the light of UV-Vis-NIR spectroscopy, dynamic light scattering (DLS) and X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM) and magnetometer SQUID analysis.

