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Properties of mechanochemically synthesized ZnS nanoparticles
E Dutková1, P Baláz, P Pourghahramani
1Institute of Geotechnics, Slovak Academy of Sciences, 043 53 Kosice, Slovakia.
Abstract:
The bulk and surface properties of mechanochemically synthesized ZnS nanoparticles were studied. XRD, SEM, TEM (HRTEM), AFM, UV-VIS, low temperature nitrogen sorption as well as TPR characterization methods have been applied. Cubic ZnS nanocrystals (2-4 nm) with characteristic blue shift have been obtained by high-energy milling. There is an evidence of the nanocrystal aggregates formation in products of milling. The surface uniformity, homogeneity as well as enhanced uptake of hydrogen have been documented.
