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Low-temperature nitridation of Fe nanoparticles precursor

H Huang1, B Lu, J P Lei

  • 1School of Materials Science and Engineering, Dalian University of Technology, Dalian, Liaoning 116024, PR China.

Journal of Nanoscience and Nanotechnology
|November 14, 2009
PubMed

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Precipitation Gravimetry01:03

Precipitation Gravimetry

Precipitation gravimetry is based on converting an analyte into a sparingly soluble precipitate, which is separated by filtration and weighed. An ideal precipitate should be pure, insoluble, of known composition, and easily filtered from the reaction mixture.
In determining nickel by gravimetric analysis, a precipitant of ethanolic dimethylglyoxime is added to a hot nickel salt solution. This is quickly followed by the dropwise addition of dilute ammonia solution until precipitation occurs. A...