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Updated: Jun 13, 2026

Synthesis and Microdiffraction at Extreme Pressures and Temperatures
Published on: October 7, 2013
Density measurement of samples under high pressure using synchrotron microtomography and diamond anvil cell
Xianghui Xiao1, Haozhe Liu, Luhong Wang
1XOR, Advanced Photon Source, Argonne National Laboratory, Argonne, IL 60439, USA.
Abstract:
Accurate mass density information is critical in high-pressure studies of materials. It is, however, very difficult to measure the mass densities of amorphous materials under high pressure with a diamond anvil cell (DAC). Employing tomography to measure mass density of amorphous samples under high pressure in a DAC has recently been reported. In reality, the tomography data of a sample in a DAC suffers from not only noise but also from the missing angle problem owing to the geometry of the DAC. An algorithm that can suppress noise and overcome the missing angle problem has been developed to obtain accurate mass density information from such ill-posed data. The validity of the proposed methods was supported with simulations.

