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Microtomographic porosity determination in alginate mixed with various methods.

Martin J Hamilton1, Kraig S Vandewalle, Howard W Roberts

  • 1United States Air Force, Advanced Education in General Dentistry Residency, Travis AFB, CA, USA.

Journal of Prosthodontics : Official Journal of the American College of Prosthodontists
|May 12, 2010
PubMed
Summary

The vacuum mixer demonstrated superior performance in reducing alginate porosities compared to centrifugal and semiautomated hand mixers. This mechanical mixing method resulted in fewer voids and smaller porosity volumes for improved dental casts.

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Area of Science:

  • Dental Materials Science
  • Biomaterials Engineering
  • Material Characterization

Background:

  • Mechanical spatulation of alginate impression materials aims to minimize voids and enhance cast quality compared to manual mixing.
  • Existing mechanical methods include vacuum mixers and semiautomated rotating bowl systems.
  • A new centrifugal-action mixer has been introduced, promising more efficient powder incorporation.

Purpose of the Study:

  • To quantitatively assess the number, percentage, and volume distribution of porosities in alginate mixed by three distinct mechanical methods.
  • To compare the efficacy of a vacuum mixer, a semiautomated hand mixer, and a new centrifugal mixer in reducing alginate porosity.
  • To utilize microtomography for a non-destructive analysis of alginate mixing-induced porosities.

Main Methods:

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  • Alginate was mechanically mixed using three methods: vacuum mixer, semiautomated hand mixer, and centrifugal mixer, following manufacturer instructions.
  • The set alginate samples were analyzed using microtomography and specialized software to quantify porosity.
  • Statistical analysis involved Kruskal-Wallis ANOVA and Mann-Whitney tests to compare porosity parameters between groups.

Main Results:

  • Significant differences (p < 0.001) in porosity number, percentage, and volume distribution were observed across the three mixing methods.
  • The vacuum mixer yielded significantly fewer porosities (both in number and percentage) compared to the centrifugal and semiautomated hand mixers.
  • Both vacuum and centrifugal mixers produced significantly smaller porosity volumes than the semiautomated hand mixer.

Conclusions:

  • The vacuum mixer exhibited the best overall performance in minimizing the number, percentage, and volume of porosities in alginate.
  • Mechanical mixing significantly impacts alginate porosity, with vacuum mixing being the most effective among the tested methods.
  • Reducing porosity in alginate impression materials is crucial for achieving superior dental cast quality.