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Updated: Jun 12, 2026

Determining the Mechanical Strength of Ultra-Fine-Grained Metals
Published on: November 22, 2021
Microstructure versus size: mechanical properties of electroplated single crystalline Cu nanopillars
Andrew T Jennings1, Michael J Burek, Julia R Greer
1Engineering and Applied Sciences, California Institute of Technology, 1200 East California Boulevard, Pasadena, California 91125, USA.
Abstract:
We report results of uniaxial compression experiments on single-crystalline Cu nanopillars with nonzero initial dislocation densities produced without focused ion beam (FIB). Remarkably, we find the same power-law size-driven strengthening as FIB-fabricated face-centered cubic micropillars. TEM analysis reveals that initial dislocation density in our FIB-less pillars and those produced by FIB are on the order of 10(14) m(-2) suggesting that mechanical response of nanoscale crystals is a stronger function of initial microstructure than of size regardless of fabrication method.

