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Real-time Monitoring of Reactions Performed Using Continuous-flow Processing: The Preparation of 3-Acetylcoumarin as an Example
Published on: November 18, 2015
A simple flowcell for reaction monitoring by NMR
M Khajeh1, M A Bernstein, G A Morris
1School of Chemistry, The University of Manchester, Manchester M13 9PL, UK.
Magnetic Resonance in Chemistry : MRC
|June 11, 2010
Abstract:
A simple, cheap and flexible flowcell based on a standard 5 mm NMR tube, designed for the monitoring of reactions but of wide applicability, is described. No modification of the NMR instrument is needed, allowing the system to be employed with any conventional NMR probe and magnet. The system is robust and economical in use of reagents, and can be used for studying both homogeneous and heterogeneous reactions.
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