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Direct conversion of urea into graphitic carbon nitride over mesoporous TiO2 spheres under mild condition

Xiao-Xin Zou1, Guo-Dong Li, Yu-Ning Wang

  • 1State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130012, China.

Chemical Communications (Cambridge, England)
|November 17, 2010
PubMed

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One of the common methods to prepare nitriles is the dehydration of amides. This method requires strong dehydrating agents like phosphorous pentoxide or boiling acetic anhydride for converting amides to nitriles. Another reagent namely, thionyl chloride also accomplishes the dehydration of amides, where amide acts as a nucleophile. The first step of the mechanism involves the nucleophilic attack by the amide on the thionyl chloride to form an intermediate. In the next step, the electron pairs...