Jove
Visualize
Contact Us

Related Concept Videos

Glassware Calibration01:11

Glassware Calibration

Accurate calibration of glassware, such as volumetric flasks, pipettes, and burettes, is essential to ensure accurate measurements in the analytical laboratory. Calibration helps maintain consistency across measurements and prevents errors arising from inaccurate volumes.
Volumetric flasks: Volumetric flasks are designed to prepare aqueous solutions of precise volumes accurately with a calibration line on the neck. To calibrate a volumetric flask, it is important to fill it with distilled...
Volatilization01:10

Volatilization

Volatilization gravimetry is an analytical technique that measures the mass lost due to the volatilization of the substance. This technique is used to estimate the amount of volatile material in a sample. To perform this method, heat a known amount of the sample to a high temperature in a crucible or other suitable vessel. The volatile substance in the sample evaporates, and the vapor is completely expelled from the crucible either by heating the sample or bubbling a stream of inert gas through...

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Purpose in life, personal growth, life satisfaction and risk of cognitive impairment among older women.

Aging & mental health·2026
Same author

The Strategic Role of 2D Nanomaterials in Grid Modernization.

ACS energy letters·2026
Same author

Characterization of Electronic Stress-Induced Changes in Multilayer MoS<sub>2</sub>.

ACS applied electronic materials·2026
Same author

Medication adherence and persistence of newly initiated medications in older adults with diabetes.

Journal of the American Pharmacists Association : JAPhA·2026
Same author

Primary care clinicians' perspectives on an electronic health record-integrated clinical decision support tool for opioid use disorder.

Journal of substance use and addiction treatment·2026
Same author

Meaning, Purpose, and Spirituality in Lifestyle Medicine and Healthcare: A Review of Current Research.

American journal of lifestyle medicine·2026
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Experiment Video

Updated: Jun 6, 2026

Sample Preparation in Quartz Crystal Microbalance Measurements of Protein Adsorption and Polymer Mechanics
08:21

Sample Preparation in Quartz Crystal Microbalance Measurements of Protein Adsorption and Polymer Mechanics

Published on: January 22, 2020

Quartz crystal microbalances for microscale thermogravimetric analysis.

Elisabeth Mansfield1, Aparna Kar, Timothy P Quinn

  • 1Materials Reliability Division, National Institute of Standards and Technology, Boulder, Colorado 80305, United States.

Analytical Chemistry
|November 18, 2010
PubMed
Summary

A novel quartz crystal microbalance (QCM) method analyzes microscale sample purity and consistency. This technique requires only micrograms of material, correlating well with traditional thermogravimetric analysis (TGA).

More Related Videos

Adsorption Device Based on a Langatate Crystal Microbalance for High Temperature High Pressure Gas Adsorption in Zeolite H-ZSM-5
09:46

Adsorption Device Based on a Langatate Crystal Microbalance for High Temperature High Pressure Gas Adsorption in Zeolite H-ZSM-5

Published on: August 25, 2016

Quantitative Analysis by Thermogravimetry-Mass Spectrum Analysis for Reactions with Evolved Gases
06:51

Quantitative Analysis by Thermogravimetry-Mass Spectrum Analysis for Reactions with Evolved Gases

Published on: October 29, 2018

Related Experiment Videos

Last Updated: Jun 6, 2026

Sample Preparation in Quartz Crystal Microbalance Measurements of Protein Adsorption and Polymer Mechanics
08:21

Sample Preparation in Quartz Crystal Microbalance Measurements of Protein Adsorption and Polymer Mechanics

Published on: January 22, 2020

Adsorption Device Based on a Langatate Crystal Microbalance for High Temperature High Pressure Gas Adsorption in Zeolite H-ZSM-5
09:46

Adsorption Device Based on a Langatate Crystal Microbalance for High Temperature High Pressure Gas Adsorption in Zeolite H-ZSM-5

Published on: August 25, 2016

Quantitative Analysis by Thermogravimetry-Mass Spectrum Analysis for Reactions with Evolved Gases
06:51

Quantitative Analysis by Thermogravimetry-Mass Spectrum Analysis for Reactions with Evolved Gases

Published on: October 29, 2018

Area of Science:

  • Analytical Chemistry
  • Materials Science
  • Nanotechnology

Background:

  • Traditional thermogravimetric analysis (TGA) requires milligram-scale samples for chemical purity and consistency analysis.
  • Microscale sample analysis presents challenges due to the limited material available.
  • Developing sensitive analytical methods for small quantities is crucial for advanced materials research.

Purpose of the Study:

  • To introduce a new method for analyzing chemical purity and consistency of microscale samples.
  • To demonstrate the utility of a quartz crystal microbalance (QCM) sensor platform for this purpose.
  • To compare the QCM method's performance against conventional thermogravimetric analysis (TGA).

Main Methods:

  • Utilized a quartz crystal microbalance (QCM) sensor platform to monitor submicrogram mass changes.
  • Deposited thin films of various materials onto the QCM sensor.
  • Analyzed mass changes as a function of temperature, mimicking TGA principles.

Main Results:

  • Achieved good correlation between QCM measurements and conventional TGA for diverse materials.
  • Successfully analyzed organic compounds, ionic detergents, powders, carbon nanotubes, and mixtures.
  • Demonstrated effective analysis with sample masses on the order of micrograms, significantly less than TGA's milligram requirement.

Conclusions:

  • The QCM sensor platform offers a highly sensitive method for analyzing microscale sample purity and consistency.
  • This approach is effective for a wide range of materials, including nanoparticles and thin films.
  • The QCM method significantly reduces the required sample mass compared to traditional TGA.