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Related Concept Videos

X-ray Crystallography02:18

X-ray Crystallography

The size of the unit cell and the arrangement of atoms in a crystal may be determined from measurements of the diffraction of X-rays by the crystal, termed X-ray crystallography.
Diffraction
Diffraction is the change in the direction of travel experienced by an electromagnetic wave when it encounters a physical barrier whose dimensions are comparable to those of the wavelength of the light. X-rays are electromagnetic radiation with wavelengths about as long as the distance between neighboring...
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There are two main infrared (IR) spectrophotometers: dispersive IR spectrometers and Fourier transform infrared (FTIR) spectrometers. In a dispersive IR spectrometer, a beam of infrared radiation produced by a hot wire is divided into two parallel equal-intensity beams using mirrors. One beam passes through the sample, while another is a reference beam. The beams then move through the monochromator, which separates the radiations into a continuous spectrum of different frequencies. The...
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X-ray diffraction or XRD is an analytical tool that utilizes X-rays to study ordered structures such as crystalline organic and inorganic samples, polycrystalline materials, proteins, carbohydrates, and drugs.
According to Bragg's law, when X-rays strike the sample positioned on a stage, the rays are  scattered by the electron clouds around the sample atoms. The  X-ray diffraction or scattering is caused by constructive interference of the X-ray waves that reflect off the internal crystal...
Phase Contrast and Differential Interference Contrast Microscopy01:26

Phase Contrast and Differential Interference Contrast Microscopy

Phase-Contrast Microscopes
In-phase-contrast microscopes, interference between light directly passing through a cell and light refracted by cellular components is used to create high-contrast, high-resolution images without staining. It is the oldest and simplest type of microscope that creates an image by altering the wavelengths of light rays passing through the specimen. Altered wavelength paths are created using an annular stop in the condenser. The annular stop produces a hollow cone of...
Determination of Crystal Structures01:29

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German physicist Wilhelm Röntgen (1845–1923) was experimenting with electrical current when he discovered that a mysterious and invisible "ray" would pass through his flesh but leave an outline of his bones on a screen coated with a metal compound. In 1895, Röntgen made the first durable record of the internal parts of a living human: an "X-ray" image (as it came to be called) of his wife’s hand. Scientists worldwide quickly began their own experiments with X-rays, and by 1900, X-ray was widely...

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Related Experiment Video

Updated: Jun 4, 2026

Measurement of X-ray Beam Coherence along Multiple Directions Using 2-D Checkerboard Phase Grating
10:39

Measurement of X-ray Beam Coherence along Multiple Directions Using 2-D Checkerboard Phase Grating

Published on: October 11, 2016

Phase measurement x-ray interferometry.

D R Schwarzenberger1, D G Chetwynd, D K Bowen

  • 1Centre for Microengineering and Metrology, Department of Engineering, University of Warwick, Coventry CV4 7AL, United Kingdom.

Journal of X-Ray Science and Technology
|February 11, 2011
PubMed
Summary
This summary is machine-generated.

This study introduces a phase-step method for x-ray interferometry, enabling precise displacement measurements with high accuracy. The technique offers improved reliability and tolerance to experimental errors for advanced scientific applications.

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Area of Science:

  • Materials Science
  • Physics
  • Metrology

Background:

  • X-ray interferometry is crucial for high-precision measurements.
  • Existing fringe analysis methods have limitations in accuracy and reliability.
  • Standard phase-plot methods require adaptation for interferometric fringe analysis.

Purpose of the Study:

  • To develop a phase-step procedure for x-ray interferometry.
  • To enable the use of standard phase-plot methods for fringe analysis.
  • To enhance the precision and reliability of displacement measurements.

Main Methods:

  • A phase-step procedure was implemented with an x-ray interferometer.
  • Standard phase-plot methods were adapted for fringe analysis.
  • Silicon (111) lattice planes were used as diffracting elements (period 0.3135625 nm).

Main Results:

  • The phase-step method allows for precise interpolation of fringe spacings.
  • The technique is more tolerant of experimental uncertainties compared to previous methods.
  • Routine displacement measurements with a standard deviation of 0.003 nm were achieved.

Conclusions:

  • The developed phase-step procedure significantly improves x-ray interferometry.
  • This method offers enhanced precision and reliability for displacement metrology.
  • The experimental and data analysis methods for achieving high resolution are detailed.