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N-Phenyl-succinamic acid.

B Thimme Gowda, Sabine Foro, B S Saraswathi

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|April 28, 2011

Summary

This summary is machine-generated.

This study details the crystal structure of C(10)H(11)NO(3), revealing specific anti and syn conformations within its amide and acid groups. Molecules form infinite chains via intermolecular hydrogen bonds in the crystal lattice.

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A Strategy for Sensitive, Large Scale Quantitative Metabolomics

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Published on: May 27, 2014

Area of Science:

Crystallography
Molecular Structure
Chemical Bonding

Background:

Understanding molecular conformations is crucial for predicting chemical properties and interactions.
Crystal structure analysis provides detailed insights into intermolecular forces and packing arrangements.

Purpose of the Study:

To elucidate the specific molecular conformations and hydrogen bonding patterns in the crystal structure of C(10)H(11)NO(3).
To describe the packing of molecules within the crystal lattice.

Main Methods:

Single-crystal X-ray diffraction was employed to determine the three-dimensional structure of the compound.
Analysis of bond orientations and intermolecular interactions (hydrogen bonds) was performed.

Main Results:

The study identified anti conformations between N-H and C=O bonds in the amide segment.
Anti conformations were observed between the amide O atom, carbonyl O atom of the acid segment, and adjacent -CH(2) groups.
Syn conformations were found between the C=O and O-H bonds of the acid group.
Infinite chains along the a axis were formed through intermolecular N-H⋯O and O-H⋯O hydrogen bonds.

Conclusions:

The crystal structure of C(10)H(11)NO(3) is characterized by specific conformational arrangements (anti and syn) of its functional groups.
Intermolecular hydrogen bonding dictates the formation of one-dimensional chains in the solid state, influencing crystal packing.