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Solid-phase Synthesis of [4.4] Spirocyclic Oximes
Published on: February 6, 2019
4-But-oxy-3-(2,4-dichloro-phen-yl)-1-oxaspiro-[4.5]dec-3-en-2-one
Liang-Zhong Xu1, Shan-Qi Sun, Wei Guo
1College of Chemistry and Molecular Engineering, Qingdao University of Science and Technology, Qingdao 266042, People's Republic of China.
Abstract:
In the title compound, C(19)H(22)Cl(2)O(3), the cyclo-hexane ring adopts a chair conformation. The furan ring plane forms dihedral angles of 81.88 (2) and 50.19 (3)°, respectively, with the benzene ring and the plane formed by the butyl C atoms. The crystal structure is stabilized by weak inter-molecular C-H⋯O hydrogen bonds.
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