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Updated: Jun 1, 2026

Continuous Flow Chemistry: Reaction of Diphenyldiazomethane with p-Nitrobenzoic Acid
Published on: November 15, 2017
4,8,9,10-Tetra-kis(4-fluoro-phen-yl)-1,3-diaza-tricyclo-[3.3.1.1]decan-6-one
Abstract:
In the title compound, C(32)H(24)F(4)N(2)O, all four six-membered rings that constitute the diaza-adamantanone cage adopt chair conformations. Two of the four fluoro-phenyl substituents occupy axial positions and the other two occupy equatorial positions relative to their respective C(5)N rings of the adamantane framework. The crystal structure is stabilized by C-H⋯O inter-actions, generating a C(5) chain along the a axis.
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