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Yong-Tao Wang¹, Xiao-Lei Chu, Shi-Chen Yan

¹Shandong Provincial Key Laboratory of Fine Chemicals, Department of Chemical Engineering, Shandong Institute of Light Industry, Jinan, Shandong 250353, People's Republic of China.

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Summary

This summary is machine-generated.

This study details the crystal structure of 1-(2-hydroxy-ethyl)-2-methyl-5-nitro-1H-imidazol-3-ium perchlorate. The compound features zigzag chains formed by intermolecular hydrogen bonds between cations.

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Area of Science:

Crystallography
Materials Science
Organic Chemistry

Background:

Understanding the crystal structure of organic salts is crucial for predicting their physical and chemical properties.
Nitroimidazole derivatives are of interest due to their diverse applications.

Purpose of the Study:

To elucidate the crystal structure of 1-(2-hydroxy-ethyl)-2-methyl-5-nitro-1H-imidazol-3-ium perchlorate.
To identify and analyze the intermolecular and intramolecular interactions within the crystal lattice.

Main Methods:

Single-crystal X-ray diffraction was employed to determine the crystal structure.
Analysis of hydrogen bonding networks (N-H⋯O, O-H⋯O, C-H⋯O) was performed.

Main Results:

The crystal structure reveals cations linked by intermolecular N-H⋯O hydrogen bonds, forming zigzag chains along the c axis.
Cations and anions are interconnected via O-H⋯O and C-H⋯O hydrogen bonds.
A weak intramolecular C-H⋯O hydrogen bond was also identified.

Conclusions:

The hydrogen bonding network significantly influences the packing and stability of the crystal structure.
The detailed structural information provides a basis for further studies on the properties and potential applications of this nitroimidazole derivative.