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Related Concept Videos

Scanning Electron Microscopy01:07

Scanning Electron Microscopy

A scanning electron microscope (SEM) is used to study the surface features of a sample by using an electron beam that scans the sample surface in a two-dimensional manner. Typically, areas between ~1 centimeter to 5 micrometers in width can be imaged. SEM can be used to image bacteria, viruses, tissues as well as larger samples like insects. Conventional SEM gives a magnification ranging from 20X to 30,000X and spatial resolution of 50 to 100 nanometers.
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Accelerated...
Electron Microscope Tomography and Single-particle Reconstruction01:07

Electron Microscope Tomography and Single-particle Reconstruction

Transmission electron microscopy (TEM) can be used to determine the 3D structure of biological samples with the help of techniques such as electron microscope tomography and single-particle reconstruction. While single-particle reconstruction can examine macromolecules and macromolecular complexes in vitro conditions only, tomography permits the study of cell components or small cells in vivo.
Electron Tomography
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Overview of Electron Microscopy01:25

Overview of Electron Microscopy

The wavelengths of visible light ultimately limit the maximum theoretical resolution of images created by light microscopes. Most light microscopes can only magnify 1000X, and a few can magnify up to 1500X. Electrons, like electromagnetic radiation, can behave like waves, but with wavelengths of 0.005 nm, they produce significantly greater resolution up to 0.05 nm as compared to 500 nm for visible light. An electron microscope (EM) can create a sharp image that is magnified up to 2,000,000X.
Transmission Electron Microscopy01:15

Transmission Electron Microscopy

In 1931, physicist Ernst Ruska—building on the idea that magnetic fields can direct an electron beam just as lenses can direct a beam of light in an optical microscope—developed the first prototype of the electron microscope. This development led to the development of the field of electron microscopy. In the transmission electron microscope (TEM), electrons are produced by a hot tungsten element and accelerated by a potential difference in an electron gun, which gives them up to 400 keV in...
Atomic Force Microscopy01:08

Atomic Force Microscopy

Atomic force microscopy (AFM) is a type of scanning probe microscopy that can analyze topographic details of various specimens like ceramics, glass, polymers, and biological samples. AFM offers over 1000 times more resolution than the optical imaging system. Images generated from AFM are three-dimensional surface profiles, offering an advantage over the flat, two-dimensional images from other imaging techniques.
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Compositional analysis with atomic column spatial resolution by 5th-order aberration-corrected scanning transmission

David Hernández-Maldonado1, Miriam Herrera, Pablo Alonso-González

  • 1Departamento de Ciencia de los Materiales e I.M. y Q.I., Facultad de Ciencias, Universidad de Cádiz, Campus Río San Pedro, s/n, 11510 Puerto Real, Cádiz, Spain. david.hernandez@uca.es

Microscopy and Microanalysis : the Official Journal of Microscopy Society of America, Microbeam Analysis Society, Microscopical Society of Canada
|May 28, 2011
PubMed
Summary

This study demonstrates atomic-resolution elemental mapping of InxGa1-xAs multilayers using aberration-corrected high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM). The results accurately map indium distribution, supporting existing segregation models.

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Quantitative Atomic-Site Analysis of Functional Dopants/Point Defects in Crystalline Materials by Electron-Channeling-Enhanced Microanalysis
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Quantitative Atomic-Site Analysis of Functional Dopants/Point Defects in Crystalline Materials by Electron-Channeling-Enhanced Microanalysis

Published on: May 10, 2021

Area of Science:

  • Materials Science
  • Nanotechnology
  • Solid State Physics

Background:

  • Characterizing the elemental composition of semiconductor heterostructures is crucial for understanding their electronic properties.
  • Accurate compositional profiling at the atomic scale is challenging but essential for advanced material design.

Purpose of the Study:

  • To demonstrate the capability of aberration-corrected HAADF-STEM for atomic-resolution elemental mapping in InxGa1-xAs multilayer structures.
  • To validate the accuracy of compositional profiles obtained from HAADF-STEM images against established segregation models.

Main Methods:

  • Utilizing 5th-order aberration-corrected high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM).
  • Analyzing HAADF-STEM images to generate elemental compositional maps and profiles.
  • Comparing experimental compositional profiles with Muraki's segregation model.

Main Results:

  • Achieved atomic-column resolution elemental compositional maps and profiles across an InxGa1-xAs multilayer.
  • Demonstrated accurate mapping of indium (In) distribution within the multilayer structure.
  • Observed good agreement between experimental results and Muraki's segregation model.

Conclusions:

  • Aberration-corrected HAADF-STEM is a powerful technique for atomic-resolution compositional analysis of semiconductor multilayers.
  • The study validates the accuracy of HAADF-STEM for characterizing indium segregation in InxGa1-xAs systems.
  • This methodology provides insights into material growth and electronic properties of quantum well structures.