Microstructure and chemical analysis of blood-contaminated mineral trioxide aggregate

M H Nekoofar1, T E Davies, D Stone

  • 1Endodontology Research Group, School of Dentistry, Cardiff University, Cardiff, UK. nekoofarmh@cardiff.ac.uk

Abstract

Insights

Blood contamination negatively impacts Mineral Trioxide Aggregate (MTA) by hindering the formation of calcium hydroxide during early hydration. This affects MTA's chemical properties and microstructure.

Area of Science:

  • Dental Materials Science
  • Biomaterials Chemistry

Background:

  • Mineral Trioxide Aggregate (MTA) is a widely used dental material.
  • Understanding factors affecting MTA's properties is crucial for clinical success.

Purpose of the Study:

  • To investigate the detrimental effects of blood contamination on the chemical properties of Mineral Trioxide Aggregate (MTA).

Main Methods:

  • Scanning electron microscopy (SEM) and energy-dispersive X-ray analysis (EDX) were used to assess microstructure and elemental chemistry.
  • X-ray diffraction analysis (XRD) evaluated phase compositions of contaminated and uncontaminated MTA.

Main Results:

  • Blood contamination altered the hydration state of MTA specimens.
  • Ettringite crystal formation was absent in blood-contaminated MTA.
  • Calcium hydroxide formation was inhibited in MTA mixed with blood.

Conclusions:

  • Blood contamination significantly interferes with the early hydration process of MTA.
  • The absence of calcium hydroxide formation indicates altered chemical properties of contaminated MTA.