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Updated: May 31, 2026
07:06
Continuous Flow Chemistry: Reaction of Diphenyldiazomethane with p-Nitrobenzoic Acid
Published on: November 15, 2017
5-(3,4-Dimethyl-benzyl-idene)-2,2-dimethyl-1,3-dioxane-4,6-dione.
1MicroScale Science Institute, Department of Chemistry and Chemical Engineering, Weifang University, Weifang 261061, People's Republic of China.
Summary
Researchers synthesized a novel compound, C(15)H(16)O(4), using 2,2-dimethyl-1,3-dioxane-4,6-dione and 3,4-dimethyl-benzaldehyde. The study reveals its crystal structure and intermolecular hydrogen bonding.
Area of Science:
- Organic Chemistry
- Crystallography
Background:
- The synthesis of novel organic compounds is crucial for developing new materials and pharmaceuticals.
- Understanding the three-dimensional structure of molecules provides insights into their properties and reactivity.
Purpose of the Study:
- To synthesize and characterize a new organic compound with the molecular formula C(15)H(16)O(4).
- To elucidate the crystal structure and intermolecular interactions of the synthesized compound.
Main Methods:
- The compound was synthesized via the reaction of 2,2-dimethyl-1,3-dioxane-4,6-dione and 3,4-dimethyl-benzaldehyde in ethanol.
- X-ray crystallography was employed to determine the molecular and crystal structure.
Main Results:
- The synthesis yielded the target compound C(15)H(16)O(4).
- The crystal structure analysis revealed an envelope conformation for the 1,3-dioxane ring.
- Weak intermolecular C-H⋯O hydrogen bonds were observed, linking molecules into chains parallel to the b axis.
Conclusions:
- A new organic compound was successfully synthesized and characterized.
- The crystal packing is stabilized by intermolecular hydrogen bonding, influencing the overall structure.
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