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Preparation and characterization of a tetrabutylammonium graphite intercalation compound

Weekit Sirisaksoontorn1, Adeniyi A Adenuga, Vincent T Remcho

  • 1Department of Chemistry, Oregon State University, Corvallis, Oregon 97331-4003, United States.

Journal of the American Chemical Society
|July 26, 2011
PubMed

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Preparation of Acid Anhydrides01:07

Preparation of Acid Anhydrides

One of the methods for preparing symmetrical or unsymmetrical acid anhydrides involves the treatment of acid chlorides with the sodium salt of carboxylic acids. The reaction proceeds via a nucleophilic acyl substitution.
The carboxylate ion acts as a nucleophile that attacks the carbonyl carbon of the acid chloride to form a tetrahedral intermediate. Subsequently, the re-formation of the carbonyl group with the loss of the chloride ion as a leaving group leads to the formation of an acid...