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Updated: May 30, 2026

Applications of Liquid-Chromatography Tandem Mass Spectrometry in Natural Products Research: Tropane Alkaloids as a Case Study
Published on: March 8, 2024
A new triterpene from Salvia xanthocheila Boiss
Somayyeh Gandomkar1, Maryam Yousefi, Zohreh Habibi
1Faculty of Science, Department of Chemistry, Shahid Beheshti University, G.C., Tehran, Iran.
Abstract:
From the chloroform extract of the aerial parts of Salvia xanthocheila, one new triterpene, together with two known diterpenes, two known flavonoids and a phytosterol was isolated. On the basis of comprehensive spectroscopic analyses, including electron ionisation mass spectra, ¹H-NMR, ¹³C-NMR, 1-D nuclear Overhauser effect, distortionless enchancement by polarisation transfer, H,H correlation spectroscopy, heteronuclear multiple quantum coherence, rotating frame Overhauser enhancement spectroscopy spectra and comparison with spectral data of known compounds, the structure of new compounds was established as 1β,3β-dihydroxy-olean-9(11),12-dienyl (1). The five known compounds (2-6) were 7α-acetoxyroyleanone, taxodione, salvigenin, apigenin-7,4'-dimethyl ether and β-sitosterol, respectively. These known structures are isolated from the aerial parts of S. xanthocheila for the first time.
