Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Experiment Video

Updated: May 30, 2026

Advances in Nanoscale Infrared Spectroscopy to Explore Multiphase Polymeric Systems
06:54

Advances in Nanoscale Infrared Spectroscopy to Explore Multiphase Polymeric Systems

Published on: June 23, 2023

Nanocomposite characterization on multiple length scales using µSAXS.

Ruipeng Li1, Sterling Cornaby, Marleen Kamperman

  • 1Cornell High Energy Synchrotron Source, Cornell University, Ithaca, NY 14853, USA.

Journal of Synchrotron Radiation
|August 25, 2011
PubMed
Summary
This summary is machine-generated.

Related Concept Videos

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Synergistic Control of Radiative Decay and Exciton Splitting Dynamics for Efficient Organic Solar Cells Processed by Non-Halogenated Solvent.

Advanced materials (Deerfield Beach, Fla.)·2026
Same author

Thulium fiber laser versus holmium:YAG laser for ureteroscopic lithotripsy: a single-center retrospective cohort study.

Frontiers in surgery·2026
Same author

Formation of Bimetallic Nanoparticles via Exsolution Using a Reducible Metal Oxide Capping Layer.

ACS nano·2026
Same author

Self-Organized Nanoplasmonic Artificial Leaf for Hot-Carrier Bioelectronic Interfaces.

Nature photonics·2026
Same author

Efficient Hybrid Mixed Ion Perovskite Photovoltaics: <i>In Situ</i> Diagnostics of the Roles of Cesium and Potassium Alkali Cation Addition.

Solar RRL·2026
Same author

Suppressing Phase Segregation and Improving Stability in Mixed-Halide Perovskites through Spinel Oxide-Directed Epitaxy.

Journal of the American Chemical Society·2026

This study demonstrates how scanning microbeam small-angle X-ray scattering (µSAXS) can assess homogeneity in nanocomposites. It reveals microphase separation in thermoset resol/poly(isoprene-block-ethylene oxide) materials.

Area of Science:

  • Materials Science
  • Polymer Science
  • Nanotechnology

Background:

  • Nanocomposites offer tailored material properties through rational synthesis.
  • Templating nanostructures onto functional materials is challenging, often leading to inhomogeneity and phase separation.
  • Characterizing nanocomposite microstructure is crucial for understanding material performance.

Purpose of the Study:

  • To investigate the homogeneity and microphase separation of a thermoset resol/poly(isoprene-block-ethylene oxide) nanocomposite.
  • To demonstrate the utility of scanning microbeam small-angle X-ray scattering (µSAXS) for multi-length scale characterization.
  • To provide insights into the templating process challenges in nanocomposite fabrication.

Main Methods:

  • Utilizing scanning microbeam small-angle X-ray scattering (µSAXS).

More Related Videos

Assembly and Characterization of Polyelectrolyte Complex Micelles
08:44

Assembly and Characterization of Polyelectrolyte Complex Micelles

Published on: March 2, 2020

Concurrent Quantitative Conductivity and Mechanical Properties Measurements of Organic Photovoltaic Materials using AFM
08:59

Concurrent Quantitative Conductivity and Mechanical Properties Measurements of Organic Photovoltaic Materials using AFM

Published on: January 23, 2013

Related Experiment Videos

Last Updated: May 30, 2026

Advances in Nanoscale Infrared Spectroscopy to Explore Multiphase Polymeric Systems
06:54

Advances in Nanoscale Infrared Spectroscopy to Explore Multiphase Polymeric Systems

Published on: June 23, 2023

Assembly and Characterization of Polyelectrolyte Complex Micelles
08:44

Assembly and Characterization of Polyelectrolyte Complex Micelles

Published on: March 2, 2020

Concurrent Quantitative Conductivity and Mechanical Properties Measurements of Organic Photovoltaic Materials using AFM
08:59

Concurrent Quantitative Conductivity and Mechanical Properties Measurements of Organic Photovoltaic Materials using AFM

Published on: January 23, 2013

  • Analyzing a thermoset resol/poly(isoprene-block-ethylene oxide) nanocomposite.
  • Characterizing material homogeneity and microphase separation across multiple length scales.

    • Main Results:

    • Scanning microbeam small-angle X-ray scattering (µSAXS) successfully characterized the nanocomposite.
    • Evidence of inhomogeneity and microphase separation was observed within the nanocomposite material.
    • The technique provided detailed microstructural information on multiple length scales.

    Conclusions:

    • Scanning microbeam small-angle X-ray scattering (µSAXS) is an effective tool for evaluating nanocomposite homogeneity.
    • The study highlights the challenges in achieving uniform nanostructure transfer during nanocomposite synthesis.
    • Understanding microphase separation is key to optimizing nanocomposite design and fabrication.