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Morpholin-4-ium hydrogen tartrate.

Ming-Liang Liu1

  • 1Ordered Matter Science Research Center, Southeast University, Nanjing 211189, People's Republic of China.

Acta Crystallographica. Section E, Structure Reports Online
|February 21, 2012
PubMed
Summary
This summary is machine-generated.

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This study details the crystal structure of a morpholinium monotartrate molecular salt. Researchers found specific conformations and hydrogen bonding patterns influencing its solid-state structure.

Area of Science:

  • Crystallography
  • Molecular structure analysis
  • Supramolecular chemistry

Background:

  • Molecular salts are crucial in various chemical applications.
  • Understanding the solid-state structure of ionic compounds is essential for predicting their properties.
  • Morpholinium and tartrate ions are common organic building blocks.

Purpose of the Study:

  • To elucidate the crystal structure of morpholinium monotartrate.
  • To investigate the conformational preferences of the morpholinium cation and monotartrate anion.
  • To identify and characterize the intermolecular interactions, particularly hydrogen bonding, within the crystal lattice.

Main Methods:

  • Single-crystal X-ray diffraction was employed to determine the molecular and crystal structure.

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  • Analysis of bond lengths, bond angles, and torsion angles provided conformational insights.
  • Hydrogen bonding networks were identified and analyzed using geometric criteria.

    • Main Results:

    • The morpholinium cation adopts a chair conformation in the solid state.
    • The monotartrate anion exhibits a C-C-C-C backbone conformation close to anti (torsion angle ~173°).
    • Two intramolecular O-H⋯O hydrogen bonds stabilize the monotartrate anion.
    • Intermolecular N-H⋯O and O-H⋯O hydrogen bonds link the ions, forming (001) sheets.

    Conclusions:

    • The crystal structure of morpholinium monotartrate is characterized by specific ionic conformations.
    • Intramolecular hydrogen bonding plays a role in the anion's conformation.
    • Extensive intermolecular hydrogen bonding dictates the formation of layered structures in the crystal.