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Stefan Merkel1, Robert Köppen, Matthias Koch
1Reference Materials, Department of Analytical Chemistry, BAM Federal Institute for Materials Research and Testing, Richard-Willstätter-Strasse 11, D-12489 Berlin-Adlershof, Germany.
Epimerization of ergotamine yielded a novel compound with a nearly planar ring C and a distorted chair conformation in ring D. Structural analysis revealed extensive N-H⋯O hydrogen bonding networks.
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