Related Experiment Video
Updated: May 23, 2026

Rapid Mix Preparation of Bioinspired Nanoscale Hydroxyapatite for Biomedical Applications
Published on: February 23, 2017
Formation of nano-phase hydroxyapatite film on TiO2 nano-network
Kang Lee1, Yeong-Mu Ko, Han-Cheol Choe
1Department of Dental Materials, School of Dentistry, MRC Center, Chosun University, Gwangju 501-759, South Korea.
Abstract:
Nano- and micro-phase HA film formed on TiO2 nano-network surface by simple electrochemical treatment. The range of lateral pore size of the network specimen was about 10-120 nm on Ti surface by anodized in 5 M NaOH solution at 0.3 A for 10 min. Nano-network TiO2 surface were formed by this anodization step which acted as templates and anchorage for growth of the HA during subsequent pulsed electrochemical deposition process at 85 degrees C. The phase and morphologies of deposits HA were influenced by the electrolyte concentration. The nano needle-like precipitates formed under low SBF concentration were identified to be HA crystals orientated parallel to the c-axis direction. Increasing electrolyte concentration, needle-like deposits transferred to the plate-like and micro plate like precipitates in the case of high SBF concentration.

