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Updated: May 19, 2026

High Pressure Single Crystal Diffraction at PX^2
Published on: January 16, 2017
The Oxford-Diamond In Situ Cell for studying chemical reactions using time-resolved X-ray diffraction
Saul J Moorhouse1, Nenad Vranješ, Andrew Jupe
1Chemistry Research Laboratory, University of Oxford, Mansfield Road, Oxford OX1 3TA, United Kingdom.
Abstract:
A versatile, infrared-heated, chemical reaction cell has been assembled and commissioned for the in situ study of a range of chemical syntheses using time-resolved energy-dispersive X-ray diffraction (EDXRD) on Beamline I12 at the Diamond Light Source. Specialized reactor configurations have been constructed to enable in situ EDXRD investigation of samples under non-ambient conditions. Chemical reactions can be studied using a range of sample vessels such as alumina crucibles, steel hydrothermal autoclaves, and glassy carbon tubes, at temperatures up to 1200 °C.
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