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A versatile detector for total fluorescence and electron yield experiments.

N Thielemann1, P Hoffmann, A Föhlisch

  • 1Institute for Methods and Instrumentation for Synchrotron Radiation Research, Helmholtz-Zentrum Berlin für Materialien und Energie GmbH, Albert-Einstein-Str. 15, 12489 Berlin, Germany. nele.thielemann@helmholtz-berlin.de

The Review of Scientific Instruments
|October 2, 2012
PubMed
Summary
This summary is machine-generated.

A novel detector combining a silicon photodiode and electron repelling meshes offers versatile detection for X-ray absorption spectroscopy. This system effectively measures both electron yield and total fluorescence yield signals.

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Area of Science:

  • Materials Science
  • Surface Science
  • Spectroscopy

Background:

  • X-ray absorption spectroscopy (XAS) is crucial for material analysis.
  • Existing detectors have limitations in versatility for different yield techniques.
  • Electron yield and total fluorescence yield are key signals in XAS.

Purpose of the Study:

  • To develop and characterize a versatile detector for XAS.
  • To enable simultaneous or selective measurement of electron yield and total fluorescence yield.
  • To assess the detector's performance using near edge X-ray absorption fine structure (NEXAFS).

Main Methods:

  • Utilized a non-coated silicon photodiode combined with electron repelling meshes.
  • Incorporated a biased copper mesh to control electron yield signal transmission.
  • Performed NEXAFS studies on thermal oxidized silicon and sapphire samples.

Main Results:

  • The detector successfully probes both electron yield and total fluorescence yield.
  • A biased copper mesh allows for suppression or transmission of the electron yield signal.
  • The detector's performance was validated through NEXAFS measurements.

Conclusions:

  • The developed detector is a versatile tool for XAS, suitable for both electron yield and total fluorescence yield measurements.
  • The biased mesh provides effective control over signal detection.
  • This technology enhances the capabilities of X-ray absorption spectroscopy analysis.