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Isolated facial and meridional tris(bipyridine)Ru(II) for STM studies on Au(111)

Alexandrina Schramm1, Christophe Stroh, Kerrin Dössel

  • 1Institute of Nanotechnology, Karlsruhe Institute of Technology (KIT), P.O. Box 3640, D-76021 Karlsruhe, Germany.

Chemical Communications (Cambridge, England)
|December 25, 2012
PubMed

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Radical substitution reactions can be used to remove functional groups from molecules. The hydrogenolysis of alkyl halides is one such reaction, where the weak Sn–H bond in tributyltin hydride reacts with alkyl halides to form alkanes. Here, the reagent Bu3SnH yields tributyltin halide as a byproduct.
The bonds formed in this reaction are stronger than the bonds broken, making it energetically favorable. The reaction follows a radical chain mechanism similar to radical halogenation reactions,...