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Updated: May 13, 2026
10:14
Synthesis and Purification of Iodoaziridines Involving Quantitative Selection of the Optimal Stationary Phase for Chromatography
Published on: May 16, 2014
Iodo-durene.
Noudjoud Hamdouni1, Ouarda Brihi, Mohamed Larbi Medjroubi
1Laboratoire de Cristallographie, Département de Physique, Université Mentouri-Constantine, 25000 Constantine, Algeria.
Acta Crystallographica. Section E, Structure Reports Online
|March 12, 2013
Summary
This study details the crystal structure of 1-iodo-2,3,5,6-tetra-methyl-benzene. The chiral molecule crystallizes in space group P212121 with minimal intermolecular interactions observed.
Area of Science:
- Crystallography
- Organic Chemistry
- Solid-State Chemistry
Background:
- Understanding the solid-state structure of organic molecules is crucial for predicting their physical and chemical properties.
- Iodinated aromatic compounds are valuable intermediates in organic synthesis and materials science.
Purpose of the Study:
- To determine the crystal structure of 1-iodo-2,3,5,6-tetra-methyl-benzene.
- To analyze the molecular geometry and intermolecular interactions in the crystalline state.
Main Methods:
- Single-crystal X-ray diffraction analysis was performed.
- The crystal structure was solved and refined using standard crystallographic software.
Main Results:
- 1-iodo-2,3,5,6-tetra-methyl-benzene crystallizes in the chiral space group P212121.
- The iodine atom exhibits a slight displacement from the mean plane of the benzene ring.
- No significant intermolecular interactions were detected in the crystal lattice.
Conclusions:
- The crystal structure provides fundamental insights into the solid-state behavior of this iodinated aromatic compound.
- The observed molecular and crystal packing are consistent with weak intermolecular forces.
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