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Updated: May 11, 2026

Synthesis and Characterization of Fe-doped Aluminosilicate Nanotubes with Enhanced Electron Conductive Properties
Published on: November 15, 2016
Iron sulfide (FeS) nanotubes using sulfurization of hematite nanowires
Dustin R Cummins1, Harry B Russell, Jacek B Jasinski
1Department of Chemical Engineering and Conn Center for Renewable Energy Research, University of Louisville, Louisville, Kentucky 40292, USA.
Abstract:
We report the phase transformation of hematite (α-Fe2O3) single crystal nanowires to crystalline FeS nanotubes using sulfurization with H2S gas at relatively low temperatures. Characterization indicates that phase pure hexagonal FeS nanotubes were formed. Time-series sulfurization experiments suggest epitaxial growth of FeS as a shell layer on hematite. This is the first report of hollow, crystalline FeS nanotubes with NiAs structure and also on the Kirkendall effect in solid-gas reactions with nanowires involving sulfurization.

