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Updated: May 6, 2026

Assessment of Labile Organic Carbon in Soil Using Sequential Fumigation Incubation Procedures
Published on: October 29, 2016
Soil sampling and analysis for volatile organic compounds.
T E Lewis1, A B Crockett, R L Siegrist
1Forestry Sciences Laboratory, U.S. Bureau of Land Management, 3041 Cornwallis Road, 27709, Research Triangle Park, NC, USA.
This guide addresses concerns about sampling soils for volatile organic compounds (VOCs). It provides techniques for sample collection, handling, and storage to minimize VOC loss and improve data quality for environmental analysis.
Area of Science:
- Environmental Science
- Analytical Chemistry
- Geology
Background:
- Data quality concerns in soil sampling for volatile organic compounds (VOCs) are prevalent among environmental professionals.
- Remedial Project Managers (RPMs) and On-Scene Coordinators (OSCs) frequently inquire about optimal sampling devices and methodologies.
Purpose of the Study:
- To provide guidance on selecting effective sampling devices for VOCs in various soil matrices.
- To address specific questions regarding VOC loss during sample transfer, container selection, and preservation techniques.
- To improve the representativeness of soil samples for volatile organic analyses (VOA).
Main Methods:
- Guidance on selecting appropriate sampling devices for VOCs in different soil types and depths.
- Description of techniques for sample collection, handling, containerization, shipment, and storage.
- Focus on methods to minimize VOC losses during all stages of the sampling process.
Main Results:
- The paper offers specific recommendations for sampling devices and techniques.
- The described methods are designed to reduce volatile organic compound (VOC) losses.
- The techniques enhance the reliability and representativeness of soil samples for VOC analysis.
Conclusions:
- Implementing the recommended sampling, handling, and storage procedures significantly reduces VOC losses.
- These improved techniques lead to more accurate and reliable volatile organic analyses (VOA) results.
- The guidance is crucial for ensuring data integrity in environmental site assessments.
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