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Updated: Apr 20, 2026

High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy
Published on: October 9, 2020
Contributed review: nuclear magnetic resonance core analysis at 0.3 T
Jonathan Mitchell1, Edmund J Fordham1
1Schlumberger Gould Research, High Cross, Madingley Road, Cambridge CB3 0EL, United Kingdom.
Intermediate field nuclear magnetic resonance (NMR) offers advanced reservoir core analysis. This technology complements low-field NMR, providing detailed porosity and pore size distribution data, especially for challenging shale formations.
Area of Science:
- Geoscience
- Petrophysics
- Analytical Chemistry
Background:
- Nuclear Magnetic Resonance (NMR) is crucial for laboratory petrophysical analysis of reservoir core plugs and fluids.
- Low-field NMR magnet technology has been historically emphasized for well log calibration.
- There is a growing interest in utilizing stronger magnets to enhance reservoir sample studies beyond standard NMR measurements.
Purpose of the Study:
- To review the capabilities of an intermediate field (0.3 T) imaging magnet for reservoir core analysis.
- To highlight the advantages of intermediate field NMR for characterizing diverse rock types, including shales.
- To demonstrate the complementary role of intermediate field NMR to low-field instruments in core analysis and materials science.
Main Methods:
- Utilized a 0.3 T imaging magnet (12.9 MHz proton frequency) for reservoir core plug analysis.
- Acquired multidimensional imaging data.
- Performed quantitative estimation of porosity, saturation, and pore size distributions.
- Investigated the detection of lower gyromagnetic ratio nuclei and employed short probe recovery times.
Main Results:
- Achieved quantitative estimates of porosity and pore size distributions, particularly effective in carbonate samples.
- Demonstrated the suitability of the system for shale studies due to advanced imaging and detection capabilities.
- Generated quantitative porosity maps of rock plugs, offering insights not achievable with high-field medical scanners due to susceptibility contrasts.
- Presented example data illustrating the utility of intermediate field imaging.
Conclusions:
- Intermediate field NMR imaging instruments provide valuable quantitative data for reservoir core analysis.
- These systems complement low-field NMR by offering multidimensional imaging and enhanced characterization, especially for shales.
- The technology holds significant potential for both petrophysical studies and broader materials science applications.
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